HCID 52943823, compound → HCID 135979913, compound

Participants

Reaction Steps

10% Pd/C was added to a solution of 37 in 95% EtOH (20 mL). The reaction mixture was stirred at ambient temperature under a H2 atmosphere for 24 h. The reaction mixture was filtered through celite and the filtrate was concentrated in vacuo. The resulting residue was triturated in 1:1 Et2O/hexane and the precipitate was collected by vacuum filtration to provide the title compound as an off-white solid. 1H NMR (DMSO-d6) δ 0.85 (t, J=7.1 Hz, 3H), 1.07 (t, J=7.1 Hz, 3H), 3.38 (m, 4H), 3.51 (q, J=7.2 Hz, 2H), 3.66 (m, 4H), 4.06 (q, J=7.1 Hz, 2H), 6.83 (m, 3H), 7.40-7.49 (m, 7H), 9.67 (s, 1H). Mass Spectrum (ESI+) m/e=516.3 (M+H).

Provenance & Evidence