Cyclopropanecarboxaldehyde → HCID 58691345, compound

Participants

Reaction Steps

N-(2-(6-(2-Acetamidobenzo[d]thiazol-4-yloxy)pyrimidin-4-yl)-5-(trifluoromethyl)phenyl)piperidine-2-carboxamide from step (a) above (0.40 g, 0.72 mmol) was reacted with cyclopropanecarboxaldehyde (0.16 mL, 2.2 mmol, Aldrich) under the conditions of Example 3(d) to give the title compound as an off-white solid. MS (ESI, pos. ion.) m/z: 611 (M+1). Mp: 212.3-213.5° C.

Provenance & Evidence