tert-Butyl methacrylate → HCID 69919662, compound
Reaction equation
[C:1]([O:6][C:7]([CH3:10])([CH3:9])[CH3:8])(=[O:5])[C:2]([CH3:4])=[CH2:3].C([O:14][CH:15]=[CH:16][C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1)(=O)C>C1(C)C=CC=CC=1>[OH:14][CH:15]=[CH:16][C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1.[C:1]([O:6][C:7]([CH3:10])([CH3:9])[CH3:8])(=[O:5])[C:2]([CH3:4])=[CH2:3]Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
Tert-butyl methacrylate (5.7 g; 40 mmol) and 9.7 g (60 mmol) of acetoxystyrene were dissolved in toluene (80 mL). The reaction product was separated by the same method as that described in example 2, except that 0.67 g of AIBN was added.
Workup
- customThe reaction product was separated by the same method as
- additionwas added
Sources & evidence
- ORD record
- ord-df255f8d76bf44bab57b0f52b41259e0
- Source dataset
- uspto-grants-2001_09
- Patent number
- US06284438B1
Reaction notes
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