HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus tribromide → HCID 53929309, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus tribromide | HCID 24614 | — |
| Reactant | HCID 54539253 | HCID 54539253 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 53929309 | HCID 53929309 | — |
Reaction Steps
A solution of 6-chloro-8-hydroxymethyl-N9-neopentylpurine (1 mmol) in methylene chloride was treated with phosphorus tribromide (1 mmol) at 25° C. for 6 h. Extraction and chromatography afforded 6-chloro-8-bromomethyl-N9-neopentylpurine as a white solid. TLC: Rf=0.64, 25% EtOAc-hexane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06284748B1 |
| Source dataset | uspto-grants-2001_09 |
| ORD ID | ord-dc20c363ddda4f2c9c04ffd4058fa2ef |
| Source note | uspto-grants-2001_09 |