化工社化工社 化学情報印刷レポート · 研究参考用
HCID 178496563、化合物 → HCID 178496562、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | HCID 178496563 | HCID 178496563 | — |
| 触媒 | Palladium | HCID 23938 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | HCID 178496562 | HCID 178496562 | 91.2% |
反応手順
A mixture of cis-3-nitro-1-(4-methoxycyclohexylmethyl)-4-methyl-2-pyridone (0.16 g, 0.57 mmol) and 10% Pd/C (0.06 g) in ethanol was hydrogenated at 50 psi in a Parr apparatus for 22 hours. The catalyst was removed by filtration, and the solvent was evaporated to give cis-3-amino-1-(4-methoxycyclohexylmethyl)-4-methyl-2-pyridone (0.13 g, 0.52 mmol, 91%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06284768B1 |
| 出典データセット | uspto-grants-2001_09 |
| ORD ID | ord-1f9f8a207409435394372a044b20aa43 |
| 出典メモ | uspto-grants-2001_09 |