Benzenesulfonyl chloride → HCID 21706749, compound

HRID 1594694Notes

Reaction equation

[C:1]1([CH:7]2[CH2:11][CH2:10][CH2:9][NH:8]2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[C:12]1([S:18](Cl)(=[O:20])=[O:19])[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1>>[C:12]1([S:18]([N:8]2[CH2:9][CH2:10][CH2:11][CH:7]2[C:1]2[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=2)(=[O:20])=[O:19])[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1

Participants

Reactant 2

HCID 7369Benzenesulfonyl chloride

HCID 2618922-Phenylpyrrolidine

Product 1

HCID 21706749HCID 21706749, compound

Procedure

The title compound, light pink solid, m.p. 116° C. and MS: m/e=287 (M+) was prepared in accordance with the general method of example 1e from (RS)-2-phenyl-pyrrolidine and benzenesulfonyl chloride.

Sources & evidence

ORD record: ord-45e7750588b74346a65f850856204991
Source dataset: uspto-grants-2001_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06284785B1

Reaction notes

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