4-Chlorobenzenesulfonyl chloride → HCID 21706696, compound

HRID 1594695Notes

Reaction equation

HRID 1594695 reaction equation
[C:1]1([CH:7]2[CH2:11][CH2:10][CH2:9][NH:8]2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[Cl:12][C:13]1[CH:18]=[CH:17][C:16]([S:19](Cl)(=[O:21])=[O:20])=[CH:15][CH:14]=1>>[Cl:12][C:13]1[CH:18]=[CH:17][C:16]([S:19]([N:8]2[CH2:9][CH2:10][CH2:11][CH:7]2[C:1]2[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=2)(=[O:21])=[O:20])=[CH:15][CH:14]=1

Participants

3

Reactant 2

HCID 73984-Chlorobenzenesulfonyl chlorideHCID 2618922-Phenylpyrrolidine

Product 1

HCID 21706696HCID 21706696, compound

Procedure

The title compound, pale pink solid, m.p. 119° C. and MS: m/e=321 (M+) was prepared in accordance with the general method of example 1e from (RS)-2-phenyl-pyrrolidine and 4-chloro-benzenesulfonyl chloride.

Sources & evidence

ORD record
ord-5283ba51571747b98ee64e5cec952958
Source dataset
uspto-grants-2001_09
Patent number
US06284785B1

Reaction notes

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