Benzenesulfonyl chloride → HCID 21706695, compound

HRID 1594702Notes

Reaction equation

HRID 1594702 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([CH:8]2[CH2:12][CH2:11][CH2:10][NH:9]2)=[CH:4][CH:3]=1.[C:13]1([S:19](Cl)(=[O:21])=[O:20])[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1>>[C:13]1([S:19]([N:9]2[CH2:10][CH2:11][CH2:12][CH:8]2[C:5]2[CH:4]=[CH:3][C:2]([Cl:1])=[CH:7][CH:6]=2)(=[O:21])=[O:20])[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1

Participants

3

Reactant 2

HCID 7369Benzenesulfonyl chlorideHCID 5923912-(4-Chlorophenyl)pyrrolidine

Product 1

HCID 21706695HCID 21706695, compound

Procedure

The title compound, white solid, m.p. 122° C. and MS: m/e=321 (M+) was prepared in accordance with the general method of example 1e from (RS)-2-(4-chloro-phenyl)-pyrrolidine and benzenesulfonyl chloride.

Sources & evidence

ORD record
ord-6fcb7393e15e4c3bbf11e9052049eca9
Source dataset
uspto-grants-2001_09
Patent number
US06284785B1

Reaction notes

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