4-Chlorobenzenesulfonyl chloride → HCID 21706776, compound

HRID 1594718Notes

Reaction equation

HRID 1594718 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([CH:8]2[CH2:12][CH2:11][CH2:10][NH:9]2)[CH:5]=[CH:6][CH:7]=1.[Cl:13][C:14]1[CH:19]=[CH:18][C:17]([S:20](Cl)(=[O:22])=[O:21])=[CH:16][CH:15]=1>>[Cl:13][C:14]1[CH:19]=[CH:18][C:17]([S:20]([N:9]2[CH2:10][CH2:11][CH2:12][CH:8]2[C:4]2[CH:5]=[CH:6][CH:7]=[C:2]([Cl:1])[CH:3]=2)(=[O:22])=[O:21])=[CH:16][CH:15]=1

Participants

3

Reactant 2

HCID 73984-Chlorobenzenesulfonyl chlorideHCID 45798062-(3-chlorophenyl)pyrrolidine

Product 1

HCID 21706776HCID 21706776, compound

Procedure

The title compound, light brown solid, m.p. 99° C. and MS: m/e=355 (M+) was prepared in accordance with the general method of example 1e from (RS)-2-(3-chloro-phenyl)-pyrrolidine and 4-chloro-benzenesulfonyl chloride.

Sources & evidence

ORD record
ord-6a12d5b9dbbf4d828cda06d529bb356e
Source dataset
uspto-grants-2001_09
Patent number
US06284785B1

Reaction notes

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