4-Chlorobenzenesulfonyl chloride → HCID 2805672, compound

HRID 1594722Notes

Reaction equation

HRID 1594722 reaction equation
[S:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[CH:6]1[CH2:10][CH2:9][CH2:8][NH:7]1.[Cl:11][C:12]1[CH:17]=[CH:16][C:15]([S:18](Cl)(=[O:20])=[O:19])=[CH:14][CH:13]=1>>[Cl:11][C:12]1[CH:17]=[CH:16][C:15]([S:18]([N:7]2[CH2:8][CH2:9][CH2:10][CH:6]2[C:2]2[S:1][CH:5]=[CH:4][CH:3]=2)(=[O:20])=[O:19])=[CH:14][CH:13]=1

Participants

3

Reactant 2

HCID 73984-Chlorobenzenesulfonyl chlorideHCID 3395542-(thiophen-2-yl)pyrrolidine

Product 1

HCID 2805672HCID 2805672, compound

Procedure

The title compound, white solid, m.p. 84° C. and MS: m/e=328.1 (M+H+) was prepared in accordance with the general method of example 1e from (RS)-2-thien-2-yl-pyrrolidine and 4-chloro-benzenesulfonyl chloride.

Sources & evidence

ORD record
ord-a6501cac5084497b92089c9c584bed61
Source dataset
uspto-grants-2001_09
Patent number
US06284785B1

Reaction notes

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