4-Chlorobenzenesulfonyl chloride → HCID 21706746, compound
Reaction equation
[O:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[CH:6]1[CH2:10][CH2:9][CH2:8][NH:7]1.[Cl:11][C:12]1[CH:17]=[CH:16][C:15]([S:18](Cl)(=[O:20])=[O:19])=[CH:14][CH:13]=1>>[Cl:11][C:12]1[CH:17]=[CH:16][C:15]([S:18]([N:7]2[CH2:8][CH2:9][CH2:10][CH:6]2[C:2]2[O:1][CH:5]=[CH:4][CH:3]=2)(=[O:20])=[O:19])=[CH:14][CH:13]=1Participants
3
Procedure
The title compound, yellow oil, MS: m/e=311 (M+) was prepared in accordance with the general method of example 1e from (RS)-2-furan-2-yl-pyrrolidine and 4-chloro-benzenesulfonyl chloride.
Sources & evidence
- ORD record
- ord-c90ea1ba1b3745a09d34090e4989f361
- Source dataset
- uspto-grants-2001_09
- Patent number
- US06284785B1
Reaction notes
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