HRID1594876

反应详情

EQUATION

反应方程式

HRID 1594876 的结构方程式

PROCEDURE

实验过程

Using the procedure described in Example 2, the crude title compound was prepared starting with 2-fluoro-4-(hydroxy-pyridin-3-yl-methyl)-benzonitrile (as described in Step C above) (0.075 g, 0.329 mmol) and 3-ethyl-3-(3-hydroxy-phenyl)-1-methyl-azepan-2-one (0.082 g, 0.329 mmol). Purification by preparative HPLC and conversion to the free base yielded the title compound.

WORKUP

后处理

  1. customthe crude title compound was prepared
  2. customPurification by preparative HPLC and conversion to the free base