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HRID1594895

反应详情

EQUATION

反应方程式

HRID 1594895 的结构方程式

REACTANTS

反应物

1
结构：Cc1ncc(CCN(C(N)=O)C(C)(C)C)n1Cc1ccc(C#N)c(F)c1
HCID21706166

未命名化合物

PRODUCTS

生成物

1
结构：Cc1ncc(CCNC(N)=O)n1Cc1ccc(C#N)c(F)c1
HCID21706187

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClCCl.O=C(O)C(F)(F)F
溶剂HCID21863450

未命名化合物

PROCEDURE

实验过程

{2-[3-(4-cyano-3-fluoro-benzyl)-2-methyl-3H-imidazol-4-yl]-ethyl}-tert-butyl urea (as described above in Step A) (0.41 g) was dissolved in TFA/CH2Cl2 3:1 (5.0 mL) and stirred at ambient temperature for 72 hr. The solvents were removed in vacuo to obtain the title compound.

WORKUP

后处理

  1. customThe solvents were removed in vacuo