Acetone → HCID 18318478, compound

HRID 1595049Notes

Reaction equation

HRID 1595049 reaction equation
Cl.[CH3:2][CH:3]([C:37]([O:39]C)=[O:38])[CH2:4][CH2:5][O:6][C:7]1[CH:36]=[CH:35][C:10]([CH2:11][C:12]2[C:13]3[CH:34]=[CH:33][CH:32]=[CH:31][C:14]=3[S:15][C:16]=2[C:17]2[CH:22]=[CH:21][C:20]([O:23][CH2:24][CH2:25][N:26]3[CH2:30][CH2:29][CH2:28][CH2:27]3)=[CH:19][CH:18]=2)=[CH:9][CH:8]=1.[OH-].[Na+].CC(C)=O>CO>[CH3:2][CH:3]([C:37]([OH:39])=[O:38])[CH2:4][CH2:5][O:6][C:7]1[CH:36]=[CH:35][C:10]([CH2:11][C:12]2[C:13]3[CH:34]=[CH:33][CH:32]=[CH:31][C:14]=3[S:15][C:16]=2[C:17]2[CH:18]=[CH:19][C:20]([O:23][CH2:24][CH2:25][N:26]3[CH2:30][CH2:29][CH2:28][CH2:27]3)=[CH:21][CH:22]=2)=[CH:9][CH:8]=1

Participants

5

Reactant 3

HCID 180AcetoneHCID 14798Sodium HydroxideHCID 18318504HCID 18318504, compound

Product 1

HCID 18318478HCID 18318478, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

The hydrolysis of the product from Example 31 was carried out at room temperature by NaOH solution using acetone and methanol as the solvent.

Sources & evidence

ORD record
ord-b4f82cf8fb19471fbd2e07676e5f35fe
Source dataset
uspto-grants-2001_09
Patent number
US06284756B1

Reaction notes

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