Carbon Dioxide → HCID 15540350, compound

HRID 1595149Notes

Reaction equation

HRID 1595149 reaction equation
[C:1](=[O:3])=[O:2].[OH-:4].[CH3:5][N+:6]1([CH3:12])[CH2:11][CH2:10][CH2:9][CH2:8][CH2:7]1>C1(C)C=CC=CC=1>[C:1](=[O:4])([OH:3])[O-:2].[CH3:5][N+:6]1([CH3:12])[CH2:11][CH2:10][CH2:9][CH2:8][CH2:7]1

Participants

4

Reactant 2

HCID 280Carbon DioxideHCID 11984246HCID 11984246, compound

Product 1

HCID 15540350HCID 15540350, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

Carbon dioxide was passed for 1 hour into 553 g of a 15.56% strength aqueous N,N-dimethylpiperidinium hydroxide solution. The solution heated up from 20° C. to 38° C. within °minutes, and then cooled down again. 300 ml of toluene was added to 100 ml of the solution. The resultant mixture was refluxed and the water was distilled off azeotropically over a period of 11 hours.

Workup

  1. temperatureThe solution heated up from 20° C. to 38° C. within °minutes
  2. temperaturecooled down again
  3. distillationthe water was distilled off azeotropically over a period of 11 hours

Sources & evidence

ORD record
ord-cd5ef3e7d01947fc9e19ccd770da0f07
Source dataset
uspto-grants-2001_09
Patent number
US06288009B1

Reaction notes

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