HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Iodide → HCID 10644565, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Iodide | HCID 5238 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 1-(4-Fluorophenyl)piperazine | HCID 75260 | — |
| Reactant | HCID 10753483 | HCID 10753483 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 10644565 | HCID 10644565 | — |
Reaction Steps
A suspension of Compound 6 (611 mg, 2.4 mmole), 1-(4-fluorophenyl)piperazine (649 mg, 3.6 mmole), potassium carbonate (498 mg, 3.6 mmole) and sodium iodide (720 mg, 4.8 mmole) in acetonitrile (30 ml) was refluxed for 38 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06288056B1 |
| Source dataset | uspto-grants-2001_09 |
| ORD ID | ord-367f5d2d35d3409eb850a7c344d0e806 |
| Source note | uspto-grants-2001_09 |