HuagongsheHuagongshe Chemistry Print Report · For research reference only
N2-((tert-Butoxy)carbonyl)-L-asparagine → 3alpha-N-(N-tert-butyloxycarbonyl-L-asparagyl)aminocholestane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N2-((tert-Butoxy)carbonyl)-L-asparagine | HCID 82035 | — |
| Reactant | 3Alpha-aminocholestane | HCID 10872780 | — |
| Product | 3alpha-N-(N-tert-butyloxycarbonyl-L-asparagyl)aminocholestane | HCID 20683735 | 56% |
Reaction Steps
By using N-tert-butyloxycarbonyl-L-asparagine (464 mg, 2.00 mmol) and 3α-aminocholestane (777 mg, 2.00 mmol), the title compound was obtained in the same manner as in Synthetic Example BB1 (670 mg, yield; 56%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06288041B1 |
| Source dataset | uspto-grants-2001_09 |
| ORD ID | ord-aa6986cf6a6e4b12b974ebeaa81a42a8 |
| Source note | uspto-grants-2001_09 |