HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzylamine → HCID 178450795, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzylamine | HCID 7504 | — |
| Reactant | HCID 178451311 | HCID 178451311 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 178450795 | HCID 178450795 | 19% |
Reaction Steps
tert-Butyl 2-hydroxyimino-3-oxo-3-(2-pyrazinyl)propionate (4.1 g) and benzylamine (4.0 g) were dissolved in acetonitrile (100 ml), and the mixture was reacted and treated in the same manner as in Starting Material Synthetic Example 5 to give tert-butyl 2-phenyl-5-(2-pyrazinyl)imidazole-4-carboxylate (1.0 g), melting point 196-197° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06288061B1 |
| Source dataset | uspto-grants-2001_09 |
| ORD ID | ord-a451dde0dbe84034b1f7705ef7bc1161 |
| Source note | uspto-grants-2001_09 |