HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuric Acid → HCID 178489040, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 178489037 | HCID 178489037 | — |
| Product | HCID 178489040 | HCID 178489040 | 63.6% |
Reaction Steps
2-(4-Aminophenyl)-5-(4-methoxyphenyl)-N-(2-thiazolyl)-imidazole-4-carboxamide (0.8 g) obtained in Example 48, sodium borohydride (0.13 g), 2.5N sulfuric acid (0.4 ml) and isopentyl aldehyde (0.3 ml) were treated in the same manner as in Example 72 to give 2-(4-isopentylaminophenyl)-5-(4-methoxyphenyl)-N-(2-thiazolyl)imidazole-4-carboxamide (0.3 g), melting point 235-239° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06288061B1 |
| Source dataset | uspto-grants-2001_09 |
| ORD ID | ord-3948d3a24bf844ddb04ae417e7c9466d |
| Source note | uspto-grants-2001_09 |