Acetic Acid → HCID 21704969, compound

Participants

Reaction Steps

0.718 g (1.4 mmole) 5-(4-[2-(2,4-dimethanesulfonyloxyphenyl)ethoxy]benzylidene)thiazolidine-2,4-dione was hydrogenated over night in 100 ml ethyl acetate and 1 ml acetic acid with 1.4 g Pd/C (10%) as catalyst. The catalyst was filtered off and the filtrate was washed with water, dried with magnesium sulfate and evaporated in vacuo to give 0.55 g (yield 76%) of the desired product.

Provenance & Evidence