Triethylamine → HCID 21704971, compound

Participants

Reaction Steps

6.0 g (30.7 mmole) methyl N-[4-(2-hydroxyethyl)phenyl]carbamate was dissolved in acetonitrile. 6.17 g (61 mmole) triethylamine and 7.0 g (61 mmole) methanesulfonyl chloride were added. The mixture was stirred until completion, then the solvent was evaporated in vacuo, water was added to the residue and the product was extracted with dichloromethane to give 7.5 g (yield 89.4%) of 4-[(methoxycarbonyl)amino]phenethyl methanesulfonate.

Provenance & Evidence