HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(4-Methoxy-phenylsulfanyl)heptanoic acid ethyl ester → 2-(4-Methoxy-phenylsulfanyl)heptanoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(4-Methoxy-phenylsulfanyl)heptanoic acid ethyl ester | HCID 54357246 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Sodium Hydroxide | HCID 14798 | — |
| Product | 2-(4-Methoxy-phenylsulfanyl)heptanoic acid | HCID 18416776 | — |
Reaction Steps
2-(4 Methoxy-phenylsulfanyl)-heptanoic acid was prepared starting with 2-(4-methoxy-phenylsulfanyl)-heptanoic acid ethyl ester (4 g, 13.5 mmol) dissolved in methanol (300 ml) and 10 N NaOH (25 ml). The resulting reaction mixture was worked up as outlined in example 1. Yield 3 g (83%). yellow oil. MS: 267.1 (M−H)−.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06288086B1 |
| Source dataset | uspto-grants-2001_09 |
| ORD ID | ord-f5247eaca3674ba88f1fdb291f3ed4cf |
| Source note | uspto-grants-2001_09 |