HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethanolamine → 2-[(2-Hydroxyethyl)(3-methoxybenzyl)amino]-1-ethanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethanolamine | HCID 8113 | — |
| Reactant | 3-Methoxybenzyl chloride | HCID 69994 | — |
| Product | 2-[(2-Hydroxyethyl)(3-methoxybenzyl)amino]-1-ethanol | HCID 5184352 | — |
Reaction Steps
2-[(2-Hydroxy-ethyl)-(3-methoxy-benzyl)-amino]-ethanol was prepared according to the general method as outlined in example 83. Starting from diethanolamine (3.1 g, 29.5 mmol) and 3-methoxybenzyl chloride (5 g, 31.9 mmol). Yield 9.28 g, (99%); yellow oil; MS: 226 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06288086B1 |
| Source dataset | uspto-grants-2001_09 |
| ORD ID | ord-ac4732e74a85494fa6a625b4f5a5ecfd |
| Source note | uspto-grants-2001_09 |