HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4-Dichlorobenzyl chloride → HCID 783950, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4-Dichlorobenzyl chloride | HCID 7609 | — |
| Reactant | Diethanolamine | HCID 8113 | — |
| Product | HCID 783950 | HCID 783950 | — |
Reaction Steps
2-[(2-Hydroxy-ethyl)-(3,4-dichloro-benzyl)-amino]-ethanol was prepared according to the general method as outlined in example 83. Starting from diethanolamine (4.84 g, 46 mmol) and 3,4-dichlorobenzyl chloride (9.0 g, 46 mmol). Yield 13.8 g (99%); colorless oil; MS: 264.3 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06288086B1 |
| Source dataset | uspto-grants-2001_09 |
| ORD ID | ord-8f985abc57c1475685f9f5c680051ed5 |
| Source note | uspto-grants-2001_09 |