HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethanolamine → HCID 784350, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethanolamine | HCID 8113 | — |
| Reactant | 4-Bromobenzyl bromide | HCID 68527 | — |
| Product | HCID 784350 | HCID 784350 | — |
Reaction Steps
2-[(4-Bromobenzyl)-(2-hydroxy-ethyl)-amino]-ethanol was prepared according to the general method as outlined in example 83. Starting from diethanolamine (22.5 g, 150 mmol). and 4-bromobenzyl bromide (25 g, 100 mmol). Yield 33.66 g, (99%); yellow oil; MS: 273.8 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06288086B1 |
| Source dataset | uspto-grants-2001_09 |
| ORD ID | ord-115080b58e264155be0841208f68c288 |
| Source note | uspto-grants-2001_09 |