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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1595944Generated: October 31, 2026

Aniline → HCID 178466652, compound

https://huagongshe.com/reaction/1595944

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAnilineHCID 6115—
ReactantHCID 86583617HCID 86583617—
SolventAcetic AcidHCID 176—
ProductHCID 178466652HCID 178466652—

Reaction Steps

The method consists of a first synthesis stage, in which a mixture of 4-acetylnaphthalic anhydride, aniline, and glacial acetic acid is heated under reflux, the reaction mixture is cooled, the precipitated gray crystals are separated by filtration, treated with hydrochloric acid solution, then with hot sodium carbonate solution, and recrystallized from acetic acid. Acetyl derivative, the 4-acetylnaphthalic acid phenylimide is obtained.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06288232B1
Source datasetuspto-grants-2001_09
ORD IDord-f85fb0b8bd20407ba31f3d319a7c6f93
Source noteuspto-grants-2001_09