HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aniline → HCID 178466652, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | HCID 86583617 | HCID 86583617 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 178466652 | HCID 178466652 | — |
Reaction Steps
The method consists of a first synthesis stage, in which a mixture of 4-acetylnaphthalic anhydride, aniline, and glacial acetic acid is heated under reflux, the reaction mixture is cooled, the precipitated gray crystals are separated by filtration, treated with hydrochloric acid solution, then with hot sodium carbonate solution, and recrystallized from acetic acid. Acetyl derivative, the 4-acetylnaphthalic acid phenylimide is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06288232B1 |
| Source dataset | uspto-grants-2001_09 |
| ORD ID | ord-f85fb0b8bd20407ba31f3d319a7c6f93 |
| Source note | uspto-grants-2001_09 |