Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Acrylamide | HCID 6579 | — |
| Reactant | tert-Butyl acrylate | HCID 15458 | — |
| Reactant | Ethanaminium, N,N,N-trimethyl-2-[(1-oxo-2-propen-1-yl)oxy]-, chloride (1:1) | HCID 162071 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | t-Butylacrylate Acrylamide | HCID 86584091 | — |
Reaction Steps
To a 500 mL round-bottom, three-neck flask fitted with a thermocouple, reflux 20 condenser, and septum was added 150 mL of isopropanol followed by 16.13 g of a 50% aqueous solution of 2-trimethylammonioethylacrylate chloride, 8.06 g of t-butylacrylate, and 8.06 g of acrylamide. The solution was purged with nitrogen for 1 hour and 0.5 g AIBN was added. The mixture was purged for ˜15 minutes until all of the AIBN dissolved. The solution was heated to 75° C. under nitrogen for 16 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06290947B1 |
|---|
| Source dataset | uspto-grants-2001_09 |
|---|
| ORD ID | ord-a49064b7d8064d6ea4e55871fecf7a5a |
|---|
| Source note | uspto-grants-2001_09 |
|---|
