2-Methylbenzothiazole → HCID 86757389, compound

HRID 1596145Notes

Reaction equation

HRID 1596145 reaction equation
[CH3:1][C:2]1[S:3][C:4]2[CH:10]=[CH:9][CH:8]=[CH:7][C:5]=2[N:6]=1.[Cl:11][CH2:12][C:13]([CH2:15]Cl)=[O:14]>>[Cl-:11].[Cl:11][CH2:12][C:13](=[O:14])[CH2:15][N+:6]1[C:5]2[CH:7]=[CH:8][CH:9]=[CH:10][C:4]=2[S:3][C:2]=1[CH3:1]

Participants

3

Reactant 2

HCID 84462-MethylbenzothiazoleHCID 107931,3-Dichloroacetone

Product 1

HCID 86757389HCID 86757389, compound

Conditions

Temperature
120 °C

Procedure

A mixture of 2-methylbenzothiazole (10 g) and 40 mL 1,3-dichloroacetone is stirred at 120° C. for 24 hours. The resulting gummy solid is triturated with ethyl acetate several times. The resulting solid is collected by suction filtration and dried under vacuum. The product is used without further purification.

Workup

  1. customThe resulting gummy solid is triturated with ethyl acetate several times
  2. filtrationThe resulting solid is collected by suction filtration
  3. customdried under vacuum
  4. customThe product is used without further purification

Sources & evidence

ORD record
ord-3c6b65c9cea44fa8ab6a492e60d2357f
Source dataset
uspto-grants-2001_09
Patent number
US06291203B1

Reaction notes

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