Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Thioacetamide | HCID 2723949 | — |
| Reactant | HCID 15433015 | HCID 15433015 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 9954385 | HCID 9954385 | — |
Reaction Steps
213 mg of 2-bromo-5-(3-trifluoromethylphenyl)indan-1-one and 48.8 mg of thioacetamide are dissolved in 10 ml of dry acetone and the solution is stirred at 0° C. for 8 h. The precipitate is filtered off with suction, washed with acetone and dried in a high vacuum. 2-Methyl-6-(3-trifluoromethylphenyl)-8,8a-dihydroindeno[1,2-d]thiazol-3a-ol hydrobromide of melting point 245-250° C. (dec.) is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06291486B1 |
|---|
| Source dataset | uspto-grants-2001_09 |
|---|
| ORD ID | ord-ed41d07bf14f4a948005372889bbdefd |
|---|
| Source note | uspto-grants-2001_09 |
|---|
