Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Bromine | HCID 24408 | — |
| Reactant | HCID 15541469 | HCID 15541469 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 18511696 | HCID 18511696 | — |
Reaction Steps
To a solution of 0.88 g of 6-acetyl-3-acetyloxy-2-ethoxycarbonylpyridine in 8.8 ml of acetic acid was added 0.19 ml of bromine dropwise, and the mixture was stirred at 75° C. for 5 minutes. Evaporation of the solvent gave 0.77 g of 6-(2-bromoacetyl)-2-ethoxycarbonyl-3-hydroxypyridine hydrobromide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06291487B1 |
|---|
| Source dataset | uspto-grants-2001_09 |
|---|
| ORD ID | ord-6bda8d62aade4238909af0bdd331cb36 |
|---|
| Source note | uspto-grants-2001_09 |
|---|
