HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl isocyanate → HCID 21701930, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl isocyanate | HCID 8022 | — |
| Reactant | 3-Amino-4-hydroxybenzonitrile | HCID 271258 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 21701930 | HCID 21701930 | 70% |
Reaction Steps
Ethyl isocyanate (7.1 g; 100 mmol) was added to a stirred solution of 2-amino-4-cyanophenol (13.4 g; 100 mmol) in MeCN (250 mL), and the resultant solution was stirred for 12 h. The precipitate was filtered off and dried (vacuum) to give the sub-title compound in a 70% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06291475B1 |
| Source dataset | uspto-grants-2001_09 |
| ORD ID | ord-eb5762c222c24837abd1d18f620f8d64 |
| Source note | uspto-grants-2001_09 |