HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanethiol → HCID 21702002, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanethiol | HCID 6343 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Reactant | HCID 21701999 | HCID 21701999 | — |
| Product | HCID 21702002 | HCID 21702002 | 69% |
Reaction Steps
[6-Methoxy-2-(4-Methoxyphenyl)benzo[b]thiophen-3-yl][4-(Trimethylacetoxymethoxy)phenyl]methanone (760 mg, 1.5 mmol) was converted to the title compound by the procedure of Example 3 using 300 mg (4.5 mmol) of ethanethiol and 600 mg (4.5 mmol) of aluminum chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06291484B1 |
| Source dataset | uspto-grants-2001_09 |
| ORD ID | ord-bb9667bbdc5a4a1db3f673a9bfb37465 |
| Source note | uspto-grants-2001_09 |