HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → 4-Benzylcyclohexanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 8-Benzyl-1,4-dioxaspiro[4.5]decane | HCID 10728293 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 4-Benzylcyclohexanone | HCID 10655235 | 105.8% |
Reaction Steps
A mixture of 28 g of 8-benzyl-1,4-dioxa-spiro[4.5]decane, 100 mL of water, 10 mL of methanol and 20 g of Amberlite™ IR-120+ was heated to reflux for 5 h. After cooling, removal of solvents under reduced pressure gave 24 g of 4-benzyl-cyclohexanone as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06291499B1 |
| Source dataset | uspto-grants-2001_09 |
| ORD ID | ord-7b973ff7c49644cdb7a30f45141d6c39 |
| Source note | uspto-grants-2001_09 |