HRID1596572

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID8476

Benzenesulfonyl chloride, 3-nitro-

C6H4ClNO4S

结构：CCOC(=O)CC(NC(=O)C(Cl)c1ccc(Cl)cc1)c1cccc(N)c1

HCID70018029

未命名化合物

PRODUCTS

生成物

结构：CCOC(=O)CC(NC(=O)C(Cl)c1ccc(Cl)cc1)c1cccc(NS(=O)(=O)c2cccc([N+](=O)[O-])c2)c1

HCID70017435

未命名化合物

PROCEDURE

实验过程

Corresponding to Example 3c, 900 mg of (5b) were reacted with 3-nitrophenylsulphonyl chloride. A solid was obtained (yield: 1.18 g).

WORKUP

后处理

customA solid was obtained (yield: 1.18 g)

来源与证据

来源类型: Open Reaction Database
ORD 记录: ord-33c116fa78a64bdbb2a6dc8b89ccec3f
来源数据集: uspto-grants-2001_09
DOI: 10.6084/m9.figshare.5104873.v1
专利: US06291503B1
来源说明: uspto-grants-2001_09

反应 SMILES

[NH2:1][C:2]1[CH:3]=[C:4]([CH:8]([NH:15][C:16](=[O:26])[CH:17]([C:19]2[CH:24]=[CH:23][C:22]([Cl:25])=[CH:21][CH:20]=2)[Cl:18])[CH2:9][C:10]([O:12][CH2:13][CH3:14])=[O:11])[CH:5]=[CH:6][CH:7]=1.[N+:27]([C:30]1[CH:31]=[C:32]([S:36](Cl)(=[O:38])=[O:37])[CH:33]=[CH:34][CH:35]=1)([O-:29])=[O:28]>>[Cl:18][CH:17]([C:19]1[CH:20]=[CH:21][C:22]([Cl:25])=[CH:23][CH:24]=1)[C:16]([NH:15][CH:8]([C:4]1[CH:5]=[CH:6][CH:7]=[C:2]([NH:1][S:36]([C:32]2[CH:33]=[CH:34][CH:35]=[C:30]([N+:27]([O-:29])=[O:28])[CH:31]=2)(=[O:37])=[O:38])[CH:3]=1)[CH2:9][C:10]([O:12][CH2:13][CH3:14])=[O:11])=[O:26]