HRID1596580

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID8476

Benzenesulfonyl chloride, 3-nitro-

C6H4ClNO4S

结构：CCOC(=O)CC(NC(=O)C(CC)c1ccccc1)c1cccc(N)c1

HCID18505398

未命名化合物

PRODUCTS

生成物

结构：CCOC(=O)CC(NC(=O)C(CC)c1ccccc1)c1cccc(NS(=O)(=O)c2cccc([N+](=O)[O-])c2)c1

HCID18505384

未命名化合物

PROCEDURE

实验过程

Corresponding to Example 3c, 3.9 g of (7b) were reacted with 3-nitrophenylsulphonyl chloride. A solid was obtained (yield: 5.0 g).

WORKUP

后处理

customA solid was obtained (yield: 5.0 g)

来源与证据

来源类型: Open Reaction Database
ORD 记录: ord-a58a8b00f0e342aababcf65b657db27d
来源数据集: uspto-grants-2001_09
DOI: 10.6084/m9.figshare.5104873.v1
专利: US06291503B1
来源说明: uspto-grants-2001_09

反应 SMILES

[NH2:1][C:2]1[CH:3]=[C:4]([CH:8]([NH:15][C:16](=[O:26])[CH:17]([C:20]2[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=2)[CH2:18][CH3:19])[CH2:9][C:10]([O:12][CH2:13][CH3:14])=[O:11])[CH:5]=[CH:6][CH:7]=1.[N+:27]([C:30]1[CH:31]=[C:32]([S:36](Cl)(=[O:38])=[O:37])[CH:33]=[CH:34][CH:35]=1)([O-:29])=[O:28]>>[N+:27]([C:30]1[CH:31]=[C:32]([S:36]([NH:1][C:2]2[CH:3]=[C:4]([CH:8]([NH:15][C:16](=[O:26])[CH:17]([C:20]3[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=3)[CH2:18][CH3:19])[CH2:9][C:10]([O:12][CH2:13][CH3:14])=[O:11])[CH:5]=[CH:6][CH:7]=2)(=[O:38])=[O:37])[CH:33]=[CH:34][CH:35]=1)([O-:29])=[O:28]