참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Ammonia | HCID 222 | — |
| 반응물 | Methyl 3-methoxy-5-methylpyrazine-2-carboxylate | HCID 21702987 | — |
| 생성물 | 3-Methoxy-5-methylpyrazine-2-carboxamide | HCID 11062776 | 87% |
반응 단계
1 g (5.5 mmol) of methyl 3-methoxy-5-methylpyrazine-carboxylate was initially charged in 15 ml (198 mmol) of NH3 (25%) and the mixture was stirred at 50° C. After concentration, 0.8 g of 3-methoxy-5-methylpyrazine-2-carboxamide was obtained. The yield was 86 percent. Other data concerning the title product was:
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US06291674B1 |
|---|
| 출처 데이터셋 | uspto-grants-2001_09 |
|---|
| ORD ID | ord-3fd488a37a2049d980cdd56963b94027 |
|---|
| 출처 메모 | uspto-grants-2001_09 |
|---|
