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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1596740Generated: October 31, 2026

HCID 131632219, compound → HCID 131722859, compound

https://huagongshe.com/reaction/1596740

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 131632219HCID 131632219—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
SolventEthyl AcetateHCID 8857—
ProductHCID 131722859HCID 13172285980%

Reaction Steps

The Boc-Gly-Phe-Leu-OBzl (1.7 g) obtained in Example 19 was dissolved in a mixed solution of ethyl acetate (30 ml) and methanol (30 ml), and added with 5% Pd-C (1.5 g) to perform catalytic reduction. The reaction mixture was filtered and the filtrate was evaporated to dryness under reduced pressure to give the title compound (1.15 g).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06291671B1
Source datasetuspto-grants-2001_09
ORD IDord-253f9d4753ac4352b9a6ab08f8028dad
Source noteuspto-grants-2001_09