HCID 178418394, compound → HCID 178434068, compound

HRID 1596766Notes

Reaction equation

HRID 1596766 reaction equation
C(ON=[C:5]([C:14]1[C:23]([CH3:24])=[C:22]2[C:17]([CH2:18][CH2:19][CH2:20][S:21]2(=[O:26])=[O:25])=[CH:16][CH:15]=1)[C:6]1[C:7]([CH3:13])=[N:8][N:9]([CH3:12])[C:10]=1[OH:11])C.[OH:27]C1NN=CC=1>>[CH3:12][N:9]1[C:10]([OH:11])=[C:6]([C:5]([C:14]2[C:23]([CH3:24])=[C:22]3[C:17]([CH2:18][CH2:19][CH2:20][S:21]3(=[O:26])=[O:25])=[CH:16][CH:15]=2)=[O:27])[C:7]([CH3:13])=[N:8]1

Participants

3

Reactant 2

HCID 178418394HCID 178418394, compoundHCID 178474516HCID 178474516, compound

Product 1

HCID 178434068HCID 178434068, compound

Procedure

Yield: 0.35 g (89% of theory) of 7-(1,3 dimethyl-5-hydroxypyrazole-4-carbonyl)-8-methyl-1,1-dioxo-thio-chroman O-ethyloxime)-5-hydroxypyrazole; 1H NMR (CDCl3): δ [ppm]=9.90 (1H, bs), 8.12 (1H, d), 7.35 (1H, d), 4.32 (2H, q), 3.65 (3H, s), 3.44 (4H, m), 2.70 (3H, s), 1.73 (3H, s), 1.38 (3H, tr).

Sources & evidence

ORD record
ord-c3c380876c96467b80f1e7b637b96df6
Source dataset
uspto-grants-2001_09
Patent number
US06291682B1

Reaction notes

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