HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Naphthol → 1-(4-Morpholinophenyl)-1-phenylprop-2-yn-1-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Naphthol | HCID 8663 | — |
| Reactant | 3(4-Morpholinophenyl)-3-phenyl-3h-naphtho[2,1-b]pyran | HCID 21698801 | — |
| Product | 1-(4-Morpholinophenyl)-1-phenylprop-2-yn-1-ol | HCID 286741 | 71% |
Reaction Steps
3(4-Morpholinophenyl)-3-phenyl-3H-naphtho[2,1-b]pyran from 2-naphthol and 1(4-morpholinophenyl)-1-phenylprop-2-yn-1-ol (yield=71% after recrystallisation from EtOAc and hexane, m.p.=186-187° C. (uncorrected), λmax in toluene=500 nm, i.e. red).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06294112B1 |
| Source dataset | uspto-grants-2001_09 |
| ORD ID | ord-671b825a9d164ec0802a317c8acee2a8 |
| Source note | uspto-grants-2001_09 |