HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86584343, compound → HCID 86584344, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86584343 | HCID 86584343 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 86584344 | HCID 86584344 | 96% |
Reaction Steps
1-Methoxyimino-7-nitro-tetralin (252 mg, 1.14 mmol) was treated with 10% Pd-C (25 mg) in MeOH (5 mL) and hydrogenated at 1 atm for 2 h. The mixture was filtered through Celite to give a yellowish solid (208 mg, 96% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06294566B1 |
| Source dataset | uspto-grants-2001_09 |
| ORD ID | ord-0a9dd496683d4b61964dab53b0d3084c |
| Source note | uspto-grants-2001_09 |