HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 2-(oxan-4-ylidene)acetate → Ethyl tetrahydropyran-4-ylacetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 2-(oxan-4-ylidene)acetate | HCID 11105795 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Ethyl tetrahydropyran-4-ylacetate | HCID 2773412 | 95.9% |
Reaction Steps
A mixture of Example 219A (1 g) and 10% Pd/carbon (100 mg) in methanol(30 mL) was stiffed under hydrogen for 3.5 h, then filtered through a pad of celite and concentrated to give 0.97 g of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06294573B1 |
| Source dataset | uspto-grants-2001_09 |
| ORD ID | ord-63d4980d7ded41cba3097ff75b5b9f93 |
| Source note | uspto-grants-2001_09 |