Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 2-Aminopyridine | HCID 10439 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | Ethyl 5-bromovalerate | HCID 84580 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 21699770 | HCID 21699770 | — |
Reaction Steps
2-Aminopyridine (3-1, 1.97 g, 20.9 mmol) in 10 mL DMF was added to a suspension of NaH (60% in oil, 1.00 g, 25 mmol) in 80 mL DMF cooled to 0° C. After warming to RT for 45 min, ethyl 5-bromopentanoate (4.2 mL, 25 mmol) was added dropwise. This mixture was heated at 75° C. overnight, then cooled to RT, diluted with EtOAc, washed with water (2×), sat. NaHCO3, and brine, dried (MgSO4), filtered and concentrated. Flash chromatography (silica, 50% then 70% EtOAc/hexane) provided 3-2 as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06294549B1 |
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| Source dataset | uspto-grants-2001_09 |
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| ORD ID | ord-b8e750caed6644049b9649beb17a6942 |
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| Source note | uspto-grants-2001_09 |
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