Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ethanol | HCID 702 | — |
| Reactant | HCID 10547108 | HCID 10547108 | — |
| Product | HCID 86754155 | HCID 86754155 | — |
Reaction Steps
HCl gas was rapidly bubbled through a suspension of acid 29-3 (4.0 g, 10.81 mmol) in EtOH (50 ml) at 0° C. for 10 minutes. The cooling bath was removed and the reaction was heated to 60° C. After 18 h, the reaction was concentrated to provide ester 29-4 as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06294549B1 |
|---|
| Source dataset | uspto-grants-2001_09 |
|---|
| ORD ID | ord-65c68501c75d43d5a27f9cedae901928 |
|---|
| Source note | uspto-grants-2001_09 |
|---|
