HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 565224, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | 2-Methyl-3-nitroaniline | HCID 11783 | — |
| Reactant | 2-Furancarbonyl chloride | HCID 68242 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 565224 | HCID 565224 | — |
Reaction Steps
A solution of 2-methyl-3-nitroaniline (1 mmol) in anhydrous diethyl ether was treated with 2-furoyl chloride (1.1 mmol) and pyridine (3.0 mmol) at 25° C. for 12 h. Extraction and chromatography afforded N-(2-furoyl)-2-methyl-3-nitroaniline as a white solid. TLC: Rf=0.41, 50% EtOAc-hexane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06294672B1 |
| Source dataset | uspto-grants-2001_09 |
| ORD ID | ord-c88ae10c258f4297afc641d1610e2695 |
| Source note | uspto-grants-2001_09 |