HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pentanoyl chloride, 4-methyl- → 2-(4-Methyl-1-oxopentyl)furan
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pentanoyl chloride, 4-methyl- | HCID 170008 | — |
| Reactant | 2-(Tributylstannyl)furan | HCID 4393688 | — |
| Catalyst | HCID 178418476 | HCID 178418476 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 2-(4-Methyl-1-oxopentyl)furan | HCID 95287 | — |
Reaction Steps
A solution of 2-tributylstannylfuran (1 mmol), 4-methylvaleroyl chloride (1.1 mmol), and PdCl2(PPh3)2 (0.05 mmol) in THF was stirred at 25° C. for 24 h. Extraction and chromatography gave 2-(4-methylvaleryl)furan.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06294672B1 |
| Source dataset | uspto-grants-2001_09 |
| ORD ID | ord-79d1b5d4d8d1416d9b45830edd9b5a29 |
| Source note | uspto-grants-2001_09 |