Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Sorbitol | HCID 5780 | — |
| Reactant | Methylenebisacrylamide | HCID 8041 | — |
| Reactant | Cyclohexane | HCID 8078 | — |
| Reactant | Ammonium Persulfate | HCID 62648 | — |
| Reactant | Methacrylamide trimethylammonium hydrochloride | HCID 21700907 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Titanium oxide (Ti3O) | HCID 162651 | — |
| Product | Glycomul S | HCID 14928 | — |
Reaction Steps
20.0 parts by weight of methacrylamide trimethylammonium hydrochloride as a main monomer of a polymer gel for a light scattering member was added to 33 parts by weight of distilled water. A solution formed by dissolving 0.1 part by weight of ammonium persulfate in 2 parts by weight of distilled water, 10.0 parts by weight of titanium oxide having an average diameter of 0.2 μm (refractive index: 2.7) as a light scattering material and 0.1 part by weight of N,N′-methylenebisacrylamide as a crosslinking agent were added to the resulting solution, to prepare a uniform solution by sufficiently stirring. The resulting dispersion solution was added, in a beaker, to a solution obtained by dissolving 1.0 part by weight of a sorbitol series surface active agent (Sorgen 50, trade name, produced by Dai-ichi Kogyo Seiyaku Co., Ltd.) as a dispersion stabilizer in 100 parts by weight of cyclohexane, followed by substituting with nitrogen, and then emulsified by stirring at a high speed with a rotary stirring blade at 10,000 rpm for 10 minutes.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06295167B1 |
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| Source dataset | uspto-grants-2001_09 |
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| ORD ID | ord-f2a03a7b3785416d8f56c6935afbad3d |
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| Source note | uspto-grants-2001_09 |
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