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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1597710Generated: October 25, 2026

Sorbitol → Glycomul S

https://huagongshe.com/reaction/1597710

Reaction equation

Participants

RoleNameHCIDCharge
ReactantSorbitolHCID 5780—
ReactantMethylenebisacrylamideHCID 8041—
ReactantCyclohexaneHCID 8078—
ReactantAmmonium PersulfateHCID 62648—
ReactantMethacrylamide trimethylammonium hydrochlorideHCID 21700907—
SolventWaterHCID 962—
SolventTitanium oxide (Ti3O)HCID 162651—
ProductGlycomul SHCID 14928—

Reaction Steps

20.0 parts by weight of methacrylamide trimethylammonium hydrochloride as a main monomer of a polymer gel for a light scattering member was added to 33 parts by weight of distilled water. A solution formed by dissolving 0.1 part by weight of ammonium persulfate in 2 parts by weight of distilled water, 10.0 parts by weight of titanium oxide having an average diameter of 0.2 μm (refractive index: 2.7) as a light scattering material and 0.1 part by weight of N,N′-methylenebisacrylamide as a crosslinking agent were added to the resulting solution, to prepare a uniform solution by sufficiently stirring. The resulting dispersion solution was added, in a beaker, to a solution obtained by dissolving 1.0 part by weight of a sorbitol series surface active agent (Sorgen 50, trade name, produced by Dai-ichi Kogyo Seiyaku Co., Ltd.) as a dispersion stabilizer in 100 parts by weight of cyclohexane, followed by substituting with nitrogen, and then emulsified by stirring at a high speed with a rotary stirring blade at 10,000 rpm for 10 minutes.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06295167B1
Source datasetuspto-grants-2001_09
ORD IDord-f2a03a7b3785416d8f56c6935afbad3d
Source noteuspto-grants-2001_09