HuagongsheHuagongshe Chemistry Print Report · For research reference only
Toluene → HCID 18931904, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Reactant | 9H-Carbazole, 9-(1-methylethyl)- | HCID 73873 | — |
| Catalyst | Zincchloride | HCID 3007855 | — |
| Product | HCID 18931904 | HCID 18931904 | 61.3% |
Reaction Steps
10.0 g (47.8 mmol) of 9-isopropylcarbazole (4b), 14.2 g (194.3 mmol) of DMF, 7.0 g (51.4 mmol) of zinc chloride, 30.0 g (195.7 mmol) of phosphorus oxychloride and 100 ml of toluene were allowed to react and after treated in the same manner as with Example 1 (1) to obtain 7.78g of 3,6-diformyl-9-isopropylcarbazole (2b).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05736284 |
| Source dataset | uspto-grants-1998_04 |
| ORD ID | ord-bf8d684c6db547088382f2bcb72dd6f6 |
| Source note | uspto-grants-1998_04 |