HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acrylamide → Isooctyl Acrylate Acrylamide Vinyl Acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acrylamide | HCID 6579 | — |
| Reactant | Benzoyl Peroxide | HCID 7187 | — |
| Reactant | Vinyl Acetate | HCID 7904 | — |
| Reactant | Isooctyl acrylate | HCID 165746 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Solvent | Ethylacetate methanol | HCID 21584119 | — |
| Product | Isooctyl Acrylate Acrylamide Vinyl Acetate | HCID 86608178 | — |
Reaction Steps
The procedure of PREPARATIVE METHOD 1 above was repeated this time employing 120.0 g isooctyl acrylate, 8.0 g acrylamide, 32.0 g vinyl acetate, 0.32 g benzoyl peroxide, 216.0 g ethyl acetate and 24.0 g methyl alcohol. The resulting polymer was diluted with the ethyl acetate/methyl alcohol mixture to 21.52% solids. The adhesive polymer had a measured inherent viscosity of 1.40 dl/g in ethyl acetate at a concentration of 0.15 g/dl. Its Brookfield viscosity was 2,300 centipoise.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05736553 |
| Source dataset | uspto-grants-1998_04 |
| ORD ID | ord-67898a20c5434b3fbef6807a4686c599 |
| Source note | uspto-grants-1998_04 |