huagongshe.com
HRID1598097

反应详情

EQUATION

反应方程式

HRID 1598097 的结构方程式

REACTANTS

反应物

2
结构：Cc1occc1C(=O)Cl
HCID2759850

2-Methylfuran-3-carbonyl chloride

C6H5ClO2

结构：Nc1ccc(C(=O)N2Cc3ccccc3Cc3ccccc32)cc1
HCID15410467

未命名化合物

PRODUCTS

生成物

1
结构：Cc1occc1C(=O)Nc1ccc(C(=O)N2Cc3ccccc3Cc3ccccc32)cc1
HCID67625920

未命名化合物

PROCEDURE

实验过程

As described for Example 9, 2-methyl-3-furanecarbonyl chloride is reacted with 5-(4-amino-benzoyl)-6,11-dihydro-5H-dibenz[b,e]azepine to give the product. Recrystallization from dichloromethanehexane gives crystals, m.p. 202°-204° C.

WORKUP

后处理

  1. customto give the product
  2. customRecrystallization from dichloromethanehexane
  3. customgives crystals, m.p. 202°-204° C.