HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-[(2-methylbenzoyl)amino]benzoyl Chloride → N-[4-[(5,6-Dihydro-7H-pyrimido[5,4-d][1]benzazepin-7-yl)carbonyl]phenyl]-2-methylbenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-[(2-methylbenzoyl)amino]benzoyl Chloride | HCID 10707441 | — |
| Reactant | 6,7-dihydro-5H-benzo[b]pyrimido[4,5-d]azepine | HCID 54396988 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | N-[4-[(5,6-Dihydro-7H-pyrimido[5,4-d][1]benzazepin-7-yl)carbonyl]phenyl]-2-methylbenzamide | HCID 67624725 | — |
Reaction Steps
As described for Example 1, 5 mmol of 4-[(2-methylbenzoyl)amino]benzoyl chloride is reacted with 5 mmol of 5,6-dihydro-7H-pyrimido[5,4-d][1]benzazepine in pyridine to give the product as a solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05736538 |
| Source dataset | uspto-grants-1998_04 |
| ORD ID | ord-5811d7715cf84f08bc9ae08a244b25df |
| Source note | uspto-grants-1998_04 |